Prep: Preheat your oven to 425 F. Line an 18 by 13 inch baking sheet with parchment paper or lightly grease a cast-iron skillet.
Make the dough: In a large bowl, whisk together flour, baking powder, baking soda, sugar and salt.
388 grams all-purpose flour, 10 grams baking powder, 2 grams baking soda, 6 grams salt, 12 grams cane sugar
Stir the sourdough discard and buttermilk together until the sourdough discard is dissolved. Set aside.
120 grams sourdough discard, 180 grams buttermilk
Rub the butter pieces into the dry ingredients (or use a pastry cutter) until all of the flour is coated in fat and the mixture resembles wet sand.
226 grams unsalted butter
Make a well in the center of the flour. Pour the sourdough mixture into the center. Stir until your mixture forms a shaggy dough.
Knead the dough: Knead the dough until all the dough appears cohesive and no dry bits of flour remain.
Laminate the dough: Transfer the dough on a lightly floured surface or a piece of parchment paper. Using a rolling pin, flatten the dough out into a ½-inch thick rectangle.
Divide the dough 3 portions, stack the dough on top of each other. Repeat.
Shape: Roll the dough out into a 9 by 7-inch rectangle. Using a bench scraper or knife, trim the edges off your dough. Cut biscuits into a 4 by 3 grid or use a 2-inch biscuit cutter to make 12 portions.
Bake: Whisk the milk and melted butter together. Using a pastry brush, brush the tops of the dough (avoid the sides).
28 grams buttermilk, 14 grams unsalted butter
Reduce oven temperature to 400 F and bake biscuits until deep golden brown on bottom and golden on top, 20–25 minutes.
Transfer the hot biscuits into a large bowl lined with a tea towel to keep them warm.
Enjoy and store: These homemade biscuits are best enjoyed fresh from the oven. But will keep well in an airtight container at room temperature for up to 3 days.